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doi: ..10.1210/jcem.81.11.8923839 [PubMed: 8923839] [CrossRef] 246

The solution was then concentrated in vacuo to remove EtOH/MeOH/water, and the residue was dissolved in EtOAc (100mL), heated in a 45 deg.C oil bath, and heptane (90mL) was slowly added